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Beilstein J. Org. Chem. 2012, 8, 1443–1451, doi:10.3762/bjoc.8.164
Graphical Abstract
Figure 1: General structure of sulfoximines 1 and one of the enantiomers of S-methyl-S-phenylsulfoximine ((S)-...
Figure 2: Structures of chiral mono- and bifunctional (bis-)thioureas that have been used as organocatalysts.
Scheme 1: Synthesis of compound (S)-3.
Scheme 2: Organocatalytic desymmetrization of the cyclic anhydride 4 with (S)-3.
Scheme 3: Attempted synthesis of sulfonimidoyl-substituted thiourea (R)-9.
Scheme 4: Synthesis of the sulfonimidoyl-containing thioureas (S)-12 and (S)-13.
Scheme 5: Syntheses of ethylene-linked sulfonimidoyl-containing thioureas (SS,SC)-18 and (RS,SC)-19.